Table 1: Crystallographic data.

Empirical formula C29H31ClN2O2Ru
Formula weight 576.08
Temperature 233(2) K
Wavelength 0.71073 Å
Crystal system Monoclinic
Space group / (no. 14)
Unit cell dimensions = 16.6035(2) Å = 90°
= 16.6935(4) Å = 105.432(2)°
= 20.0607(4) Å
Volume5359.77(18) Å3
8
Density (calculated)1.428 g/cm3
Absorption coefficient0.713 mm−1
(000)2368
Crystal size0.34 × 0.15 × 0.09 mm3
Theta range for data collection1.27 to 24.94°
Index ranges , ,
Reflections collected30131
Independent reflections9334 [ (int) = 0.0359]
Reflections [ > 2sigma( )]7629
Completeness to theta = 24.94°99.6%
Absorption correctionNone
Refinement methodFull-matrix least-squares on
Data/restraints/parameters9334/6/665
Goodness-of-fit on 1.037
Final indices [ > 2sigma( )] ,
indices (all data) ,
Largest diff. peak and hole0.428 and −0.784 e Å−3