Research Article
Synthesis and Crystal Structure of trans-Diiodobis(piperidine-1-carbonitrile)platinum(II)
Table 1
Crystallographic details for trans-[PtI2(NCNC5H10)2].
| Empirical formula | C12H20I2N4Pt | Fw | 669.21 | Temp. (K) | 100(2) | () | 0.71073 | Cryst syst | Monoclinic | Space group | 21/c | a () | 6.7497(7) | b () | 15.8212(16) | c () | 8.2773(8) | (deg) | 104.110(4) | () | 857.25(15) | Z | 2 | (Mg/m3) | 2.593 | (Mo K) (mmā1) | 11.779 | Number of reflections | 27391 | Unique reflections | 4203 | GOOF (F2) | 1.229 | | 0.0257 | R1a () | 0.0160 | wR2b () | 0.0377 |
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R1 = . wR2 = [/ ]1/2.
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