Journal of Crystallography / 2014 / Article / Tab 1

Research Article

Synthesis and Structural Study of the (N,N,N′,N′-Tetraethylethylenediamine)CdFe(CO)4 Dimer

Table 1

Crystal and experimental data.

Empirical formulaC28H48Cd2Fe2N4O8
Formula weight905.20
Temperature (K)150(1) K
Wavelength (Å)0.71073 Å
Crystal systemMonoclinic
Space groupP21/a
Unit cell dimensions
14.8546(2)
15.1647(3)
15.5252(3)
(°)90.9517(12)
Volume (Å3)3496.81(11)
4
(g cm−3)1.719
(MoKα) (mm−1)2.062
(000)1824
range (°)2.62–27.46
Limiting indices−19 ≤ ≤ 19
−19 ≤ ≤ 18
−20 ≤ ≤ 20
Reflections collected/unique13001/7974
Completeness (%)99.6%
Goodness of fit on 1.034
indices [ > ( )] = 0.0380, = 0.0899
indices (all data) = 0.0530, = 0.0988
( )max, min1.847, −1.238
(int)0.0198

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