Table 1: Crystal data and the refinements details.

Empirical formula LiNa5K3Mo11As3O45
Crystal system/space group/ Triclinic/P-1/2
(Å)10.550(2)
(Å)11.723(2)
(Å)17.469(3)
α (°)102.35(3)
β (°)87.61(2)
γ (°)111.03(3)
3) 1986.46(2)
μ (mm−1) 6.39
(g·cm−3)/formula weight (g/mol)3.78/2247.34
Crystal size (mm)/Color0.2 × 0.3 × 0.5/yellow
Tmin/Tmax 0.7026/0.8745
Measured reflections 9789
Independent reflections/rint8557/0.0157
Observed refl. with > 2σ( ) 7730
Data/restraints/parameters 8557/2/619
[ > 2σ( )] 0.028
( )/ / (000)0.071/1.22/2072
Δρmax/Δρmin (e·Å−3)1.56/−1.39