Synthesis, Characterization, and X-Ray Structure of Bis(O-butyldithiocarbonato)bis(3-ethyl pyridine)nickel(II)

Table 3

Crystal and experimental data.

Empirical formula	C24H36N2NiO2S4
Formula weight	571.50
Temperature	293(2) K
Wavelength	0.71073 ́Å
Unit cell dimensions
𝑎, ́Å	14.0721(6)
𝑏, ́Å	7.0078(2)
𝑐, ́Å	15.3604(7)
𝛼, °	90.00
𝛽, °	108.065(5)
𝛾, °	90.00
𝑍	2
Space group	𝑃21/n
Crystal system	monoclinic
Calculated density, g/cm^−3	1.318
Absorption coeff., mm^−1	0.986
𝐹(000)	604
Crystal size mm	0.30×0.20×0.10
Color	Green
Theta range for entire data collection	3.43–29.07 deg.
Limiting indices	−17≤ℎ≤17, −8≤𝑘≤8, −18≤𝑙≤18
Refinement method	Full matrix least squares on 𝐹^2
Reflections collected	14671
Used in refinement	1984
Parameters	167
Goodness-of-fit on 𝐹^2	1.045
𝑅 indices	𝑅1=0.0545, 𝑤𝑅1=0.1293
Largest diff. peak and hole	0.79 and −0.42 eÅ^−3

CCDC 956444 contain the supplementary crystallographic data for this paper. The data can be obtained free of charge via http://www.ccdc.cam.ac.uk/data_request/cif by e-mailing [email protected], or by contacting The Cambridge Crystallography Data Centre, 12 Union Road, Cambridge, CB2 IEZ, UK. Fax: [phone].