Table of Contents
Journal of Crystallography
Volume 2014, Article ID 745074, 6 pages
http://dx.doi.org/10.1155/2014/745074
Research Article

Synthesis, Characterization, and Crystal Structure of Negundoside (2′-p-Hydroxybenzoyl Mussaenosidic Acid)

1Department of Physics & Electronics, University of Jammu, Jammu 180 006, India
2Indian Institute of Integrative Medicine, Jammu, India

Received 25 February 2014; Accepted 17 April 2014; Published 25 May 2014

Academic Editor: Mehmet Akkurt

Copyright © 2014 Suresh Sharma et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Abstract

The structure of title compound Negundoside (2′-p-hydroxybenzoyl mussaenosidic acid) was established by spectral and X-ray diffraction studies. The compound crystallizes in the monoclinic crystal system with space group P21 having unit cell parameters: (5) Å, (4) Å, (5) Å, (4)°, and . The crystal structure was solved by direct method using single crystal X-ray diffraction data collected at room temperature and refined by full-matrix least-squares procedures to a final R value of 0.0520 for 3389 observed reflections.