Table of Contents
Journal of Crystallography
Volume 2014, Article ID 862067, 9 pages
http://dx.doi.org/10.1155/2014/862067
Research Article

Crystal Structure, Spectral Studies, and Hirshfeld Surfaces Analysis of 5-Methyl-5H-dibenzo[b,f]azepine and 5-(4-Methylbenzyl)-5H-dibenzo[b,f]azepine

1Department of Studies in Physics, University of Mysore, Manasagangotri, Mysore 570006, India
2Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysore 570006, India
3Department of Studies in Microbiology, University of Mysore, Manasagangotri, Mysore 570006, India

Received 30 September 2013; Revised 8 December 2013; Accepted 14 February 2014; Published 19 May 2014

Academic Editor: Lígia R. Gomes

Copyright © 2014 Madan Kumar Shankar et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Linked References

  1. P. Panneerselvam, K. Sandya, and K. Vijayalakshmi, “Dibenazoazepine, a pharmacologically active moiety,” ISOR Journal of Applied Chemistry, vol. 1, no. 6, pp. 41–44, 2012. View at Google Scholar
  2. B. W. Rockliff and E. H. Davis, “Controlled sequential trials of carbamazepine in trigeminal neuralgia,” Archives of Neurology, vol. 15, no. 2, pp. 129–136, 1966. View at Google Scholar · View at Scopus
  3. H.-J. Möller, H.-P. Volz, I. W. Reimann, and K.-D. Stoll, “Opipramol for the treatment of generalized anxiety disorder: a placebo-controlled trial including an alprazolam-treated group,” Journal of Clinical Psychopharmacology, vol. 21, no. 1, pp. 59–65, 2001. View at Publisher · View at Google Scholar · View at Scopus
  4. P. C. Fuenfschilling, W. Zaugg, U. Beutler et al., “A new industrial process for oxcarbazepine,” Organic Process Research and Development, vol. 9, no. 3, pp. 272–277, 2005. View at Publisher · View at Google Scholar · View at Scopus
  5. M. P. Sadashiva, B. H. Doreswamy, Basappa, K. S. Rangappa, M. A. Sridhar, and J. S. Prasad, “Synthesis and crystal structure of 5-allyl-5H-dibenzo[b,f]azepine,” Journal of Chemical Crystallography, vol. 35, no. 3, pp. 171–175, 2005. View at Publisher · View at Google Scholar · View at Scopus
  6. H. Honda and M. B. Allen, “The effect of an iminostilbene derivative (G32883) on peripheral nerves,” Journal of the Medical Association of Georgia, vol. 62, no. 2, pp. 38–42, 1973. View at Google Scholar · View at Scopus
  7. N. A. Patil, H. S. Somashekar, S. Narendranath, P. Prashanth, S. K. Reddy, and A. Bhandarkar, “Evaluation of anticonvulsant activity of magnesium oxide alone and along with carbamazepine,” Asian Journal of Pharmaceutical and Clinical Research, vol. 5, no. 2, pp. 142–145, 2012. View at Google Scholar
  8. R. Li, C. Trankle, K. Mohr, and U. Holzgrabe, “Hexamethonium-type allosteric modulators of the muscarinic receptors bearing lateral dibenzazepine moieties,” Archiv der Pharmazie, vol. 334, no. 4, pp. 121–124, 2001. View at Google Scholar
  9. R. A. Al-Qawasmeh, Y. Lee, M.-Y. Cao et al., “11-phenyl-[b,e]-dibenzazepine compounds: novel antitumor agents,” Bioorganic and Medicinal Chemistry Letters, vol. 19, no. 1, pp. 104–107, 2009. View at Publisher · View at Google Scholar · View at Scopus
  10. M. M. M. Abdoh, S. Madan Kumar, K. S. Vinay kumar, B. C. Manjunath, M. P. Sadashiva, and N. K. Lokanath, “5-(prop-2-yn-1-yl)-5H-dibenzo[b,f]-azepine: orthorhombic polymorph,” Acta Crystallographica E, vol. 69, p. o17, 2013. View at Google Scholar
  11. B. C. Manjunath, K. S. Vinay Kumar, S. Madan Kumar, M. P. Sadashiva, and N. K. Lokanath, “5-[(4-benzyl-1H -1,2,3-triazol-1-yl)methyl]-5H -dibenzo[b,f ]azepine,” Acta Crystallographica E, vol. 69, p. o1233, 2013. View at Google Scholar
  12. S. Madan Kumar, B. C. Manjunath, G. S. Lingaraju, M. M. M. Abdoh, M. P. Sadashiva, and N. K. Lokanath, “A Hirshfeld surface analysis and crystal structure of 2′-[1-(2-fluoro-phenyl)-1H-tetrazol-5-yl]-4-methoxy-biphenyl-2-carbaldehyde,” Crystal Structure Theory and Applications, vol. 3, pp. 124–131, 2013. View at Google Scholar
  13. Apex2 (Version 2013), Program for Bruker CCD X-Ray Diffractometer Control, Bruker AXS Inc., Madison, Wis, USA, 2013.
  14. G. M. Sheldrick, “A short history of SHELX,” Acta Crystallographica A, vol. 64, no. 1, pp. 112–122, 2008. View at Publisher · View at Google Scholar · View at Scopus
  15. C. F. Macrae, I. J. Bruno, J. A. Chisholm et al., “Mercury CSD 2.0—new features for the visualization and investigation of crystal structures,” Journal of Applied Crystallography, vol. 41, no. 2, pp. 466–470, 2008. View at Publisher · View at Google Scholar · View at Scopus
  16. S. K. Wolff, D. J. Grimwood, J. J. McKinnon, D. Jayatilaka, and M. A. Spackman, CrystalExplorer 3.0, University of Western Australia, Perth, Australia, 2001.
  17. M. A. Spackman and J. J. McKinnon, “Fingerprinting intermolecular interactions in molecular crystals,” CrystEngComm, vol. 4, no. 66, pp. 378–392, 2002. View at Google Scholar
  18. M. A. Spackman, J. J. McKinnon, and D. Jayatilaka, “Electrostatic potentials mapped on Hirshfeld surfaces provide direct insight into intermolecular interactions in crystals,” CrystEngComm, vol. 10, no. 4, pp. 377–388, 2008. View at Publisher · View at Google Scholar · View at Scopus
  19. D. Jayatilaka, D. J. Grimwood, A. Lee et al., TONTO—A System for Computational Chemistry, The University of Western Australia, Nedlands, Australia, 2005.
  20. D. Cremer and J. A. Pople, “A general definition of ring puckering coordinates,” Journal of the American Chemical Society, vol. 97, no. 6, pp. 1354–1358, 1975. View at Google Scholar · View at Scopus