Research Article
Synthesis of 14-Aryl-14H-dibenzo[a,j]xanthene Derivatives Using H-Zeolite A as an Efficient and Reusable Catalyst under Solvent-Free Condition
Table 4
Comparison of H-Zeolite A for the synthesis of 14-(4-chlorophenyl)-14H-dibenzo[a,j]xanthene.
| Entry | Catalyst | Condition | Time (h) | Yield (%) | Ref. |
| 1 | H2SO4 | AcoH/80°C | 73 | 60 | [24] | 2 | Silica H2SO4 | S.f./80°C | 15–120 min | 80–96 | [28] | 3 | Amberlyst-15 | S.f./125°C | 0.5–2 | 80–94 | [30] | 4 | Yb(OTf)3 | (13py) Bf4 | 5–7 | 80–95 | [36] | 5 | NaHSO4 | S.f./90°C | 0.5–1 | 74–91 | [32] | 6 | Cellulose H2SO4 | S.f./110°C | 1.5–3 | 81–97 | [37] | 7 | H-Zeolite A | S.f./100°C | 15–35 min | 94–98 | This work |
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S.f.: solvent free.
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