Reexamination of Solvothermal Synthesis of Layered Carbon Nitride

Figure 5

The variation of the main XRD peaks at around 27° of the products obtained at various heating durations. ((a) and (b)) d-value and FWHM of the three deconvoluted peaks; diamond: s-triazine ring alignment of structural framework of cyanuric chloride 310 peak, square: s-triazine ring interlayer plane 002 peak, and triangle: heptazine ring interlayer plane 002 peak. (c) Intensity ratio of each 002 peak from the interlayer planes of s-triazine ring and heptazine ring ().

(a)

(b)

(c)