Research Article
Ecofriendly and Facile One-Pot Multicomponent Synthesis of Thiopyrimidines under Microwave Irradiation
Table 2
Melting point and TLC report of synthesized compounds 4(a–g).
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| Comp. code | R | M.F | M.W. | mp (°C) | |
| 4a | H | C11H7N3OS | 229.25 | 285–287 | 0.36 | 4b | –4F | C11H6FN3OS | 247.24 | 195–197 | 0.37 | 4c | –2Cl | C11H6ClN3OS | 263.70 | 185–187 | 0.51 | 4d | –3Cl | C11H6ClN3OS | 263.70 | 275-276 | 0.37 | 4e | –4Cl | C11H6ClN3OS | 263.70 | 205–207 | 0.32 | 4f | –3Br | C11H6BrN3OS | 308.15 | 250–252 | 0.35 | 4g | –4Br | C11H6BrN3OS | 308.15 | 242–244 | 0.40 |
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