Research Letter

C s 2 C O 3 /[bmim]Br as an Efficient, Green, and Reusable Catalytic System for the Synthesis of N-Alkyl Derivatives of Phthalimide under Mild Conditions

Table 2

Synthesis of N-alkyl phthalimides using C s 2 C O 3 /[bmim]Br catalytic system.

419054.tab.002a

R P r o d u c t a Time (min)Yield ( % ) b

C H 3 C H 2 1a 9098
C H 3 ( C H 2 ) 2 C H 2 1b 9098
C H 3 ( C H 2 ) 4 C H 2 1c9097
C 6 H 5 C H 2 1d 10096
C 6 H 5 C H 2 C H 2 1e 10096
C 6 H 5 CH=CHC H 2 1f10095
o-C H 3 O- C 6 H 4 OC H 2 CH(OH)C H 2 1g13093
C 6 H 5 1h 7096
419054.tab.002b1i 7094

a A l l compounds are known and their structures were identified by comparison of their melting points and spectral data with those in the authentic samples. b I s o l a t e d yield.