Table of Contents
Textures and Microstructures
Volume 28 (1996), Issue 1-2, Pages 71-79

The Effects of Strain Annealing on Grain Boundary Distribution and Hardening in Superpure Nickel

Department of Materials Engineering, University of Wales Swansea, Singleton Park, Swansea SA2 8PP, UK

Received 10 March 1996

Copyright © 1996 Hindawi Publishing Corporation. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.


Electron backscatter diffraction is applied to the study of texture and mesotexture in superpure nickel. Low level strain annealing is shown to influence the grain boundary population such that greater proportions of special boundaries exist. It is found that variations in the texture of a specimen are not reflected by characteristic changes in the grain boundary population, indicating that texture analysis cannot be applied to the prediction of special boundary densities. Mechanisms active during the evolution of special boundaries are discussed and compared to those involved under similar conditions in commercially pure nickel. It is shown that alnnealing twin formation need not be prevalent for a high level of special boundaries to form. Differences in the hardness of various boundary types are identified, such that low angle boundaries and ∑3 boundaries close to exact misorientation can be categorized separately to other boundaries, in that they show minimal hardening.