Research Article

Estimation of Volatile Organic Compounds (VOCs) and Human Health Risk Assessment of Simulated Indoor Environment Consisting of Upholstered Furniture Made of Commercially Available Foams

Table 2

Thermal desorption and GC-MS parameters used in the study.

Thermal desorptionShort Path Thermal Desorption Controller model TD–4, Serial J210

Temperature and time conditions of thermal desorption
OperationTime (s)Temperature [°C]
Gas purge time300
Injection time30
Desorption time180200 (initial)–250 (final)
GC start delay30
Gas chromatographAgilent Technologies GC 6890 Network GC System
Mass spectrometryAgilent Technologies GC 6890 Network GC System

Thermostat
Initial temp [°C]40
Initial time [min]2
Temperature rise rate [°C.min−1]Final temp [°C]Final time [min]
Ramp824020
Run time [min]474747

Front Inlet
ModeSplit
Temp [°C]250
Pressure [kPa]62,9
Split ratio40:1
Split flow [mL.min−1]47,9
Total flow [mL.min−1]52,6
Gas typeHelium

Column
Capillary column type:AGILENT HP–5MS (5% Phenyl methyl siloxane)
Max. temperature [°C]325
Nominal length [m]30
Nominal diameter [µm]250
Nominal film thickness [µm]1
Initial flow [mL.min−1]1,2
Average velocity [cm.sec-1]40
Nominal init pressure [kPa]63
OutletMSD
Outlet pressurevacuum

Zone MS
MS Quad–temp [°C]150 (max 200)
MS Source–temp [°C]230 (max 250)
Acquisition ModeSCAN/SIM
Low mass25
High mass500
Threshold50