Bioinorganic Chemistry and Applications / 2010 / Article / Tab 1

Research Article

Hydrogen-Bonded Networks Based on Cobalt(II), Nickel(II), and Zinc(II) Complexes of N,N'-Diethylurea

Table 1

Crystal data and structure refinement for 14.

Compound1234

Empirical formulaC30H72B2CoF8N12O6C30H72CoCl2N12O14C30H72NiCl2N12O14C30H72ZnCl2N12O14
Formula weight929.52954.81954.59961.26
Crystal size0.10 × 0.20 × 0.200.10 × 0.15 × 0.200.10 × 0.15 × 0.200.10 × 0.20 × 0.20
Crystal systemmonoclinictriclinictriclinictriclinic
Space groupP21/cP P P
θ range for data1.85 ≤ ≤ 25.001.93 ≤ θ ≤ 25.001.76 ≤ θ ≤ 25.001.76 ≤ θ ≤ 25.00
collection. °
a, Å9.495(3)13.341(5)9.063(3)9.092(6)
b, Å22.063(7)11.935(4)11.951(6)11.978(9)
c, Å12.615(4)9.052(3)13.357(6)13.370(10)
, ° 90101.925(12)114.54(2)114.34(2)
, °109.932(11)100.871(11)100.74(2)100.91(2)
, °90114.455(10)102.03(2)102.07(2)
V, Å32484.6(14)1221.3(7)1225.1(9)1233.7(15)
Z2111
, g cm-31.2421.2981.2941.294
, mm-10.4230.5280.5720.672
GOF1.0241.0541.0541.055
0.06150.05710.05700.0817
wR20.19780.17230.17990.2533

.

We are committed to sharing findings related to COVID-19 as quickly as possible. We will be providing unlimited waivers of publication charges for accepted research articles as well as case reports and case series related to COVID-19. Review articles are excluded from this waiver policy. Sign up here as a reviewer to help fast-track new submissions.