Diorganotin Complexes of a Thiosemicarbazone, Synthesis: Properties, X-Ray Crystal Structure, and Antiproliferative Activity of Diorganotin Complexes

Table 1

X-ray crystal data and structure refinement.

	5
Empirical formula	C21 H22N4O2S2Sn
Formula weight	545.24
Temperature/ (K)	100 (2)
Wavelength/ (A)	0.71073
Crystal system	Triclinic
Space group	P-1
𝑎 (Å)	9.4663 (4)
𝑏 (Å)	14.7350 (7)
𝑐 (Å)	16.6374 (7)
𝛼 (°)	94.871 (4)
𝛽 (°)	96.434 (4)
𝛾 (°)	90.793 (4)
Volume (A^3)	2297.1 (2)
𝑍	4
Dc (Mg/m^3)	1.577
Absorption coefficient (mm^-1)	1.319
F(000)	1096
Crystal size (mm)	0.32×0.28×0.16
Diffractometer	Kuma KM4CCD
Theta range for data collection (°)	3.14–36.65
Ranges of h, k, l	−15→15, −24→20, −27→27
Reflections collected	35235
Independent reflections (Rint)	18670 (0.0381)
Completeness to 2𝜃 = 36.65	81.9%
Data/parameters	18670/541
Goodness-of-fit (𝐹^2)	0.920
Final R1/wR2 indices [I>2𝜎(I)]	0.0336/0.0768
Largest diff. peak/hole (e/Å^3)	2.090/−1.098