Synthesis, Crystal Structure, and Spectra Properties of the Cadmium (II) Complex with Bis(N-allylbenzimidazol-2-ylmethyl)benzylamine
Table 1
Crystallographic data and data collection parameters for [Cd(babb)2](pic)2.
Complex
[Cd(babb)2](pic)2
Molecular formula
C70H62CdN16O14
Molecular weight
1463.76
Crystal system
Triclinic
Space group
P-1
a (Å)
13.903 (4)
b (Å)
14.146 (4)
c (Å)
19.330 (5)
α (°)
90.595 (3)
β (°)
110.890 (3)
γ (°)
106.325 (3)
V (Å3)
3382.5 (16)
Z
2
(mg m−3)
1.437
F(000)
1508
Crystal size (mm)
0.40 × 0.38 × 0.30
θ range for data collection (°)
2.25 to 25.00
h/k/l (max, min)
−16, 16/−15, 16/ −22, 22
Reflections collected
20103
Independent reflections
11730 [R(int) = 0.0253]
Completeness to theta = 25.00
98.4%
Refinement method
Full-matrix least- squares on
Data/restraints/parameters
11730/49/910
Goodness-of-fit on
1.008
Final R1, R2 indices []
0.0473, 0.1117
R1, wR2 indices (all data)
0.0682, 0.1249
Largest differences peak and hole (e Å−3)
0.986 and −0.537
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