Synthesis, Characterization and In Vitro Antibacterial Studies of Organotin(IV) Complexes with 2-Hydroxyacetophenone-2-methylphenylthiosemicarbazone (H₂dampt)

Table 1

Summary of crystal data and structure refinement parameters for ligand (1).

Compound	H2dampt (1)
Empirical formula	C16H17N3OS
Formula weight	299.39
Temperature (K)	100 (2)
Wavelength (Å)	0.71073
Crystal system	Monoclinic
Space group	P21/c
Unit cell dimensions
a (Å)	14.6966(8)
b (Å)	7.3586(4)
c (Å)	14.0926(8)
α (°)	90.00
β (°)	94.358(5)
γ (°)	90.00
Volume (Å^3)	1519.66(15)
Z	4
Calculated density (mg/m3)	1.309
Radiation type λ (Å)	Mo K⧵a
F (000)	632
Crystal size (mm)	0.30 × 0.1 × 0.05
Crystal colour	Light-yellow
Scan range θ (°)	2.8–29.3
Absorption coefficient (μ) (mm-1)	0.225
Max. and min. transm	1.00 and 0.419
Goodness of fit on F2	0.995
Data/restrains/ parameters	3375/3/201
Final R indices [I > 2σ(I)]	𝑅1 = 0.0599, 𝑤𝑅2 = 0.1324
R indices (all data)	𝑅1 = 0.110, 𝑤𝑅2 = 0.1738