Synthesis and Characterization of Bioactive Acylpyrazolone Sulfanilamides and Their Transition Metal Complexes: Single Crystal Structure of 4-Benzoyl-3-methyl-1-phenyl-2-pyrazolin-5-one Sulfanilamide

Table 1

Crystal data for 2.

Compound	Bmpp-Sn
Formula	C23H20N4O3S·H2O
Crystal colour and form	Orange/block
Formula weight	450.52
Crystal system	Monoclinic
Space group	C2/c
	23.3366 (4) (Å)
	14.7706 (3) (Å)
	12.5787 (2) (Å)
	90 (2)°
	100.727 (2)°
	4257.21 (13) ()
	8
	1.406 (Mg cm^−1)
	1888
range	2.2–28.3 (°)
Crystal size	0.24 0.38 0.56 (mm)
Reflections measured	19945
Independent/observed	5285/4408
Mu(MoKa)	0.71073 (/mm)
Temperature	296 (K)
Parameters	108