Cu(II) and Ni(II) Complexes with New Tridentate NNS Thiosemicarbazones: Synthesis, Characterisation, DNA Interaction, and Antibacterial Activity

Table 1

Summarized crystallographic data.

Compound	Melting point (°C)
Empirical formula	C13H13N5S
Mr (g·mol^−1)	271.34
Temperature (K)	298
Crystal system	Triclinic
Space group
Crystal size (mm)	0.100 × 0.250 × 0.348
a (Å)	5.8565 (2)
b (Å)	10.0980 (4)
c (Å)	11.4853 (4)
α (°)	77.2761 (13)
β (°)	86.6013 (12)
γ (°)	89.7176 (12)
V (Å^3)	661.36 (4)
Z	2
θ range	2.44 to 25.35
Dcalc (kg·m^−3)	1.363
Refined parameters	179
Total reflections	2391
Unique reflections	1875
R1 [I > 2σ(I)]	0.0548
wR2	0.1436
Goodness of fit	1.071