Research Article

Synthesis of 1,5-Benzodiazepine and Its Derivatives by Condensation Reaction Using H-MCM-22 as Catalyst

Table 2

Synthesis of 1,5-benzodiazepines and its derivatives using H-MCM-22 through a condensation reaction between a series of OPDA and various ketones.

EntryDiamineKetoneProductTime (min)Yield (%)

1510650.tab.002a6087
2510650.tab.002b6085
3510650.tab.002c6086
4510650.tab.002d5088
5510650.tab.002e6069
6510650.tab.002f12085
7510650.tab.002g12078
8510650.tab.002h 120 81