BioMed Research International / 2019 / Article / Tab 4

Research Article

Pinelliae Rhizoma Praeparatum Cum Alumine Extract: Sedative and Hypnotic Effects in Mice and Component Compounds

Table 4

Chemical components of PRPCA.

No.Rt(min)M+H+/M-H-(m/z)1Relative abundance2 (%)FormulaIdentificationComponent type

10.49175.1055/0.846276C6N4O2L-arginineAlkaloid
20.51134.0433/1.543210C4H7NO4Aspartic acidAlkaloid
30.53173.2322/20.549580C9O39-Oxo-nonanoic acidFatty acid
40.53104.0692/1.931501C4H9NO2r-Aminobutyric acidAlkaloid
50.5590.0647/1.324170C3H7NO2AlanineAlkaloid
60.55116.0694/0.667065C5H9NO2ProlineAlkaloid
70.56/
0.56
343.1393/
341.1121
17.502990/
9.261898
O8ConiferinPhenylpropanoid
80.56127.0395/0.696933C6H6O35-HydroxymethylfurfuralAlkaloid
90.56127.0395/0.527680C5H6N2O25-Methyl uracilAlkaloid
100.56181.0703/1.971326C9H8O4Caffeic acidOther
110.56/
0.55
145.0491/
143.0344
2.031063
/1.082930
C6H8O41,6:3,4-Dianhydro-β-D-allosepOther
120.56/
0.56
343.122/
341.122
17.562720
/9.233400
SucrosePhenylpropanoid
130.57148.0641/0.975707C5H9NO4Glutamic acidAlkaloid
140.60118.0849/2.538829C5NO2ValineAlkaloid
150.68137.0473/1.513341C5H4N4O6- purineAlkaloid
160.69182.0808/1.184787C9NO3TyrosineAlkaloid
170.69150.0623/0.796495C5O2NSMethionineAlkaloid
180.71132.101/2.489048C6NO2IsoleucineAlkaloid
190.71136.0645/3.803266C5H5N5Pedatisectine BAlkaloid
201.28166.0844/6.800080C9NO2PhenylalanineAlkaloid
211.29120.0781/1.324174C4H9NO3ThreonineAlkaloid
221.30167.0919/0.527678O25-Amyl-2-pyroneVolatile oil
231.30268.1042/2.220231N5O4AdenosineAlkaloid
241.50/
4.06
263.1381/
261.1375
1.702509/
1.738387
N2O3Cyclo-(Val-L-Tyr)Alkaloid
253.35696.538/1.403823NO81-O-glucosyl-N-2′-palmitoyl-4,8-sphingodienineCerebroside
263.5997.0749/1.652728C6H8O2-Ethenyl butenalVolatile oil
27/3.68/167.04211.766885C8H8O4Vanillic acidOther
284.18/
5.32
255.0653/
253.0549
2.359618
/4.502707
O4ChrysophanolAnthraquinone
295.51/191.07980.911941Methyl phenanthreneVolatile oil
305.72269.0709/1.553166N4O5InosineAlkaloid
31/7.11/329.237129.182100O5Pinellic acidFatty acid
32/14.05/293.183440.609860O4GingerolOther

Note 1: Data to the left of “/” represent the m/z of [M+H]. Data to the right of “/” represent the m/z of [M-H]. Note 2: Relative abundance values were obtained via normalization.

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