Research Article

An UPLC-MS/MS Method for Simultaneous Quantification of the Components of Shenyanyihao Oral Solution in Rat Plasma

Table 4

Precision and accuracy of the components in rat plasma sample.

CompoundsConcentration (ng/ml)Intraday ()Interday ()
Precision (RSD%)Accuracy (RE%)Precision (RSD%)Accuracy (RE%)

Stachydrine10.004.17-6.933.51-5.79
250.006.162.355.180.19
2000.001.922.692.363.49
Danshensu2.008.51-1.417.742.93
50.004.3710.5110.31-0.86
400.000.258.543.603.97
Chlorogenic acid0.205.42-7.995.25-3.25
5.003.229.481.8410.40
40.000.299.971.5611.60
Protocatechuic acid0.205.492.874.434.77
5.000.585.732.607.88
40.001.9310.721.759.02
Plantamajoside0.103.916.674.784.19
2.500.483.246.59-4.58
20.001.996.384.650.70
Aesculetin0.201.848.455.951.74
5.001.0410.082.098.26
40.000.846.872.918.75
Isoquercitrin0.202.614.583.534.19
5.001.015.030.985.00
40.000.7610.591.319.82
Ferulic acid2.007.845.396.913.39
50.001.237.271.206.40
400.000.425.691.484.06
Baicalin10.004.77-3.664.74-4.40
250.004.32-9.604.50-8.16
2000.003.08-1.174.21-5.10
Baicalein2.003.87-5.685.62-5.18
50.001.67-8.814.15-6.67
400.004.07-4.664.54-4.53