Involvement of Muscarinic Receptors in Hypotensive and Diuretic Effects of Aqueous Soluble Fraction from Asphodelus tenuifolius Cav.

Table 1

Constituents identified from aqueous soluble fraction from Asphodelus tenuifolius by LC-DAD-MS/MS.

Peak	RT (min)	Compound	UV (nm)	MF	Positive mode (m/z)
					MS [M + H]^+	MS/MS
1	1.1	Hexitol	—	C6H14O6	183.0861	91
2	1.2	di-O-hexoside	—	C12H22O11	365.1037^a
3	1.3	Tri-O-hexoside	—	C18H32O16	527.1554^a	365
4	1.3	Valine	—	C5H11NO2	118.0863	101
5	1.4	Unknown	—	C16H26N2O11	423.1618	254, 244, 224, 196
6	2.2	Adenosine	268	C10H13N5O4	268.1056	136, 119
7	2.8	Unknown	—	C16H26N2O10	407.1672	394, 369, 355, 309, 297, 271, 254
8	4.8	Peganine (vasicine)	285	C11H12N2O	189.1028	171, 143, 118, 140
9	5.0	di-O-hexosyl pegamine	280	C23H32N2O11	513.2060	351, 189, 118
10	7.0	di-O-hexosyl pegamine	280	C23H32N2O11	513.2067	351, 189, 118
11	7.9	Unknown	—	C32H44O14	675.2612	607, 417, 351
12	11.7	Tri-O-hexosyl quercetin	265, 355	C33H40O22	789.2087	465, 303
13	11.9	Tri-O-hexosyl luteolin	265, 342	C33H40O21	773.2158	449, 287
14	13.3	Unknown		C16H23NO5	310.1659	251, 207, 175, 147
15	14.7	6,8-Di-C-hexosyl apigenin	280, 332	C27H30O15	595.1637	505, 475, 433, 403, 379, 355, 337, 325
16	15.0	Unknown	—	C26H35NO9	506.2357	452, 413, 376, 298, 221
17	23.8	Tri-O-hexosyl O-deoxyhexosyl O-methyl apigenin	270, 338	C40H52O24	917.2947	447, 285, 270

RT: retention time; MF: molecular formula; ^a: [M + Na]⁺.