Role of Episamarcandin in Promoting the Apoptosis of Human Colon Cancer HCT116 Cells through the PI3K-Akt Signaling Pathway

Table 4

The ¹H-NMR and¹³CNMR parameters of episamarcandin.

	H^1NMR	^13CNMR
1	1.44 (1H, m, H-1′a)	161.4 (C-2)
2	2.08 (1H, m, H-1′b)	113.8 (C-3)
3	1.87 (1H, m, H-2′a)	144.4 (C-4)
4	1.80 (1H, m, H-2′b)	129.9 (C-5)
5	3.56 (1H, dd, J = 11.2, 4.0 Hz, H-3′)	113.6 (C-6)
6	1.16 (1H, brd, J = 12.0 Hz, H-5′)	163.4 (C-7)
7	1.95 (1H, m, H-6′a)	102.4 (C-8)
8	1.74 (1H, d, J = 12.0 Hz, H-6′b)	157.0 (C-9)
9	1.78 (1H, ov., H-7′a)	113.3 (C-10)
10	2.03 (1H, m, H-7′b)	38.8 (C-1′)
11	1.59 (1H, d, J = 4.5 Hz, H-9′)	28.5 (C-2′)
12	4.08 (1H, dd, J = 14.4, 7.2 Hz, H-11′a)	78.6 (C-3′)
13	4.33 (1H, d, J = 9.6 Hz, H-11′b)	40.1 (C-4′)
14	1.49 (3H, s, H-12′)	55.7 (C-5′)
15	1.37 (3H, s, H-13′)	19.3 (C-6′)
16	1.16 (3H, s, H-14′)	43.8 (C-7′)
17	1.32 (3H, s, H-15′)	71.6 (C-8′)
18	6.34 (1H, d, J = 9.6 hz, H-3)	59.3 (C-9′)
19	7.69 (1H, d, J = 9.6 hz, H-4)	38.7 (C-10′)
20	7.45 (1H, d, J = 8.8 hz, H-5)	68.0 (C-11′)
21	7.05 (1H, d, J = 8.8 hz, H-6)	32.0 (C-12′)
22	7.12 (1H, brs, H-8)	29.6 (C-13′)
23		17.1 (C-14′)
24		17.2 (C-15′)