Abstract

The resistivity index is an important parameter for determining the rock saturation index. However, the saturation index changes greatly in unconventional reservoirs, which leads to oil saturation estimation with great difficulty. Hence, we try to establish the relationship between the resistivity index and log data. Firstly, a novel model of estimating the resistivity index with time was derived based on fractal theory, the relationship between nuclear magnetic resonance (NMR) spectrum and capillary pressure curve (-), and Archie formula. It regards the logarithm of the resistivity index as the dependent variable, with time and time when water saturation is 100% as the independent variables. Second, 17 cores were drilled, and spectrum and the relationship between the resistivity index and water saturation (-) were jointly measured. Next, the experimental results were substituted into the established model to get the model parameters via the multivariate statistics regression method. Then, the experimental data engaged and not engaged in modeling were used to test the established model. The average relative errors of estimated resistivity indices and experimental results are smaller than 8%, and those of the regressed saturation index are smaller than 5%. Finally, the established model was applied in log data processing and interpretation with good effects. It thus proves that the method of the estimating resistivity index with time is reliable, which provides a novel solution for determining rock electrical parameter of unconventional reservoirs.

1. Introduction

The saturation model has always been a puzzle troubling petrophysicists. In the classical rock saturation model, the saturation index has always been an indispensable parameter [13]. It is obtained by regression of the - relationship. Therefore, the accurate resistivity index is very important.

In previous researches, the saturation index is usually obtained through the measured - relationship by regression [46]. One saturation index is used in the same studied interval. This way of acquiring results features high accuracy and witnesses good application effect in conventional reservoirs. However, as the main research object turns to unconventional reservoirs, the complicated lithology and pore structure lead to wider variation range of the saturation index. Moreover, the rock electrical experiment becomes more difficult, and the unified saturation index by experiment will bring great error to the evaluation of oil saturation [7]. Hence, in recent years, petrophysicists try to establish the relationship between the resistivity index and well log data, for the purpose of continuously calculating the saturation index.

The basis of the method is that there is certain relationship between the pore structure and conductive property of the rock [810]. According to the Archie formula, the resistivity index can be expressed as the quantitative function of water saturation. Meanwhile, previous researches indicate that capillary pressure can also be expressed as the function of wetting-phase saturation. It can either be the linear relationship based on the capillary model [11], or the power function relationship by fractal theory [12, 13]. Besides, Longeron et al. also carried out experimental analysis on this [14]. According to fractal theory, Ge et al. acquired the relationship between the resistivity index and capillary pressure (-) through experimental data fitting [15]. However, it was not applied in log data processing and interpretation. As a result, it is feasible to try to establish the - relationship [12, 13]. Although capillary pressure is only an experimental data, the reconstruction of pseudocapillary pressure curve with NMR data has been a very mature technology [16, 17]. Therefore, petrophysicists are also trying to establish the relationship between the resistivity index and time for realizing the estimation of the resistivity index via log data [1820].

In order to obtain the relationship mentioned above, the model of the estimating resistivity index using time and time when water saturation is 100% was first derived based on fractal theory, - relationship, and Archie formula. Then, the cores acquired from the study area were analyzed, and the above model is calibrated by the experimental data. Finally, the modeling data, the data not engaged in modeling, and the actual log data were used to test the application effect of the model, respectively, from three aspects.

2. Methodology

2.1. Geological Background

Ordos basin, located in North China (Figure 1(a)), is a sedimentation basin and rich in oil and gas resources [22]. According to basement property, tectonic evolution, and current tectonic pattern of the basin, it can be divided into 6 first-order tectonic units (Figure 1(b)). The internal structure is relatively simple with a stable formation and the inclination angle less than 1° generally, while the disrupted fold is relatively developed along the margin of the basin [2325]. The study area is at the lower-middle parts of the border between Tianhuan depression and North Shaanxi slope, which extends from Dingbian county in the north to Zhenyuan county in the south and stretches from Mahuang mountain in the west to Youfangzhuang village in the east across the Tianhuan depression tectonic belt (Figure 1(b)). The study area is the Chang 8 stratum, being the main pay zone of Triassic Yanchang formation (Figure 1(c)). In the sedimentation stage of Chang 8 stratum, it is located at a relatively stable structural environment—a typical shallow water delta sedimentation. The distribution of the sand body has a characteristic that partial thick sand body along the direction of the river channel is distributed in a cuspate shape. The fine sandstone, siltstone, and mudstone are the main lithology. The porosity and permeability are within the range of 6%-14% and , respectively, which belongs to a typical tight sandstone reservoir.

2.2. Estimation of the - relationship based on NMR spectrum

Based on fractal theory, Toledo et al. and Li and Williams considered that rock resistivity bears the following relationship with the corresponding wetting-phase saturation [12, 13]: where refers to rock resistivity, Ω•m; refers to water (wetting-phase) saturation, %; refers to a model coefficient, irrelevant to water film thickness and dimensionless; refers to fractal dimension, dimensionless.

Besides, Toledo et al. and Li and Williams together considered that the wetting-phase saturation of the rock and the corresponding capillary pressure satisfy the fractal theory [12, 13], as shown in the following relationship: where indicates the capillary pressure, MPa.

There have been a lot of publications to discuss how to reconstruct capillary pressure curve by using spectrum based on the former research results, and the technique seems to run smoothly [2628]. Scholars believe that on the premise of fixed wetting-phase saturation [17], there is an obvious power function relationship between the and time, as shown in Eq. (3):

where indicates the transversal relaxation time, ms; and mean the model coefficient, which are dimensionless.

Equation (1), Eq. (2), and Eq. (3) have been verified by petrophysical experimental results in different study areas. Equation (4) can be obtained in combination of Eq. (1), Eq. (2), and Eq. (3) under the fixed wetting-phase saturation. where is a constant, dimensionless.

Equation (4) reflects that the rock resistivity and time conform to the relationship mentioned above with the fixed wetting-phase saturation. Therefore, when the wetting-phase saturation is 100%, Eq. (4) can be expressed as Eq. (5). where indicates the corresponding time under water-saturated condition, ms; refers to the rock resistivity under water-saturated condition, Ω•m.

Equation (6) can be obtained by combining Eq. (4) and Eq. (5) under the fixed wetting-phase saturation.

where indicates the model coefficient, which is dimensionless; indicates the corresponding time under the fixed wetting-phase saturation, ms.

According to the Archie formula [(1)], the resistivity index can be expressed by Eq. (7). where indicates the resistivity index, which is dimensionless.

In fact, in the water-saturated state, equals to (), which have similar physical significance. Hence, at this time, is an independent variable. However, in other states, the value of is related to petrophysical properties of rock, and it becomes dependent.

Under the fixed saturation, substitute Eq. (6) into Eq. (7) and take the same logarithm based on 10 on both ends of the new equation to obtain Eq. (8).

For the convenience of parameter regression, we define where and indicate the model coefficient, which is dimensionless.

Equation (11) can be obtained by combining Eq. (8), Eq. (9), and Eq. (10). There is a linear relationship between lg () and lg () with as slope and as intercept obviously. where and are obtained directly by model fitting between the raw data of the spectrum and the values of .

3. Results and Discussions

3.1. Experimental Data

To establish the quantitative relationship between the resistivity index and spectrum, 17 sandstone cores (D1, D2…D17) were drilled in the study area. After processing, core plungers with length of about 4 cm and diameter of 1 inch were formed, respectively. They are complete and strong bonding with no fragmentation. The distribution scopes of porosity and permeability are 6.03%-14.13% and μm2, respectively. NaCl solution was prepared based on the average salinity of formation water as the experimental water. After the preparation of experimental materials, the cores were saturated with experimental water. The spectra under water-saturated condition were measured by the MARAN DRX2 experiment device manufactured by Oxford Instruments. The experimental data are shown in Figure 2. Then, the resistivity indices under different water saturations by gas displacing water were measured. As shown in Figure 3, the saturation indices obtained by regression based on the power function are distributed in 1.47-2.16. It reflects that the measured saturation index is of large change scope, and great errors can be caused if the average value is taken in the study area.

3.2. Determination of the Time when the Water Saturation Is 100%

According to Eq. (11), it will have a great influence on the model accuracy to acquire the accurate time when the water saturation is 100%. In Figure 2, each NMR curve represents a core under the condition of saturated water. The integrals of these NMR curves were computed from small time to big time that correspond with the -axis, which reflected the amount of pore water is more and more. Convert the measured spectrum into a cumulative curve (Figure 4) on the basis of the experimental results in Figure 2. As shown in the position indicated by the arrow, read the corresponding value on the -axis when the value of the -axis is 100%. This value is namely the corresponding time when the water saturation is 100%.

3.3. Model Establishment

During experimental measurement, the - in Figure 3 is different from the sampling point on the cumulative curve of spectrum in Figure 4. Hence, unify the sampling points of the two figures prior to the model establishment. Set a fixed water saturation value. Then make statistics, respectively, for the resistivity index in correspondence to different water saturation in Figure 3 and the time in correspondence to different water saturation in Figure 4. Take logarithm based on 10, respectively, to form a data set for calibrating the model established in Eq. (11).

After the establishment of data set, draw the 3D scatter diagram to present visually. As shown in Figure 5, -axis, -axis and -axis represent, respectively, the value of three parameters after taking the logarithm. It is obvious that in a three-dimensional space, data points form in a similar but not exactly the same tendency under different water saturations. When the water saturation is reduced, the data point is more scattered relatively. Therefore, substitute the data point under different water saturations in Figure 5 into Eq. (11), respectively. Obtain the model parameters and under different water saturations by multivariate statistics regression [22]. As shown in Table 1, the related coefficients of the model are greater than 0.8, indicating a better fitting effect and higher model accuracy.

According to the above theoretical model analysis, experimental data presentation (Figure 5), and models established (Table 1), there is a quantitative relationship as shown in Eq. (11) and Table 1 among the resistivity index, the time of corresponding saturation, and the time when the water saturation is 100%. The proposed models are supported by the modeling data.

3.4. Model Test

To test the reliability of models established in Table 1, this paper sets forth from two aspects. First, judge the resistivity indices of cores involved in the model establishment with the established models. Then, estimate the resistivity index and saturation index of cores not involved in the model establishment with the established models.

As can be seen from Figures 2 and 3, the experimental results of 17 cores were used for modeling based on Table 1. Under the condition of fixed water saturation, time and time when the water saturation is 100% in the modeling data set were, respectively, substituted into the models established in Table 1 to estimate the resistivity indices of 17 cores under different water saturation states. Then, the estimated resistivity indices and the measured results were analyzed by cross plot, as shown in Figure 6. The ordinate refers to the estimated resistivity index, and the abscissa refers to the measured one. When water saturation is less than 80%, most of the data points are distributed near the diagonal, which indicates that the estimated resistivity indices are close to the experimental results. When the water saturation is 95%, a small amount of estimated results is significantly different from the measured results, which may be the interference caused by measurement error. Table 2 lists the average values and average relative errors between the estimated and measured resistivity indices under the condition of fixed water saturation. As seen from the table, the average values are very consistent, and the average relative errors are less than 8%, indicating that the estimated results are consistent with the measured ones.

Figure 7(a) shows the spectrum experimental results of 3 cores not used for modeling. First, the spectra in Figure 7(a) were converted into the cumulative distribution curves by the order of water saturation from low to high. time corresponding to the set water saturation (95%, 80%, 65%, 50%) and time when the water saturation is 100% on the cumulative distribution curve were read, respectively. Then, they were, respectively, substituted into Table 1 to calculate the resistivity indices under different water saturation states. As shown in Figures 7(b)–(d), the estimated and measured - relationships were analyzed by cross plot; wherein, the three figures represent cores V1, V2, and V3, respectively. As can be seen from them, the estimated data points (red) almost coincide with the measured data points (blue), indicating both results are in high consistency. In addition, the regressed and measured rock electrical parameter and saturation index are shown in Table 3. The estimated results of the no matter rock electrical parameter or saturation index are in high consistency with the measured results, showing that the relative error is basically below 5%.

Whether through the experimental results involved in modeling or the ones not involved in modeling, the test results of the model are good, indicating that the estimation model established is reliable.

3.5. Analysis of the Application Effect

The above results show that the established estimation model of the resistivity index is reliable from the point of view of the core. Now it is analyzed with actual log data from a water layer. Figure 8 is a log interpretation result of well B in the study area. In the figure, the first track is the lithologic logs (natural gamma ray curve, spontaneous potential curve, and caliper curve); the second one is the porosity logs (density curve, neutron porosity curve, and acoustic curve); the third one is the resistivity logs (deep, medium, and shallow resistivity curves); the fifth one is the porosity curve calculated by density log data; the sixth one is the NMR log curve; the seventh one is time calculated when the water saturation is 100%; the eighth one is the - relationship curve; and the ninth one is the saturation index curve. Among them, the black curves in the eighth and ninth tracks are the results estimated by the established model, and the red curves and scatter points in both tracks are the analysis results of the core experiment. As seen from Figure 8, the - relationship curves estimated in the eighth track have the same trend as the analysis results of the core experiment, with similar curve shape and good coincidence. The errors between the predicted and measured saturation indices in the ninth track are very small.

To sum up, it is feasible to estimate the resistivity index by spectrum. Furthermore, the established estimation model is reliable.

4. Conclusions

Based on fractal theory, - relationship, and Archie formula, a corresponding model is derived, which regards the logarithm of the resistivity index as the dependent variable and regards time and time when the water saturation is 100% as the independent variable. The model parameters under different water saturation states were obtained by the multivariate statistical regression method, in combination with the NMR spectra and - relationships of 17 cores in the study area. Then, the reliability of the models was verified by experimental results of modeling data and nonmodeling data, with errors of less than 8% and 5%. Finally, the processing and interpretation results of the actual log data further verify the good application effect of the models. It thus proves that the method of the estimating resistivity index with time is reliable, which provides a novel solution for determining the rock electrical parameter of unconventional reservoirs.

Nomenclature

:Deep lateral resistivity, can measure the undisturbed formation, Ω·m
:Rock resistivity under water-saturated condition, Ω·m
:Water saturation, %
:Fractal dimension, dimensionless
:Capillary pressure, Mpa
:The index of pore structure related to formation factors by Archie formula, dimensionless
:The saturation index associated with the resistance increase index in The Archie formula, dimensionless
:Transverse relaxation time used to characterize the decay of the NMR spin-echo signal, s
:Corresponding T2 time under water-saturated condition, s
:Resistivity index in Archie formula, dimensionless
, , , :The parameters of models, dimensionless.

Data Availability

The data used but not presented in the manuscript will be provided on request.

Conflicts of Interest

The authors declare that they have no conflicts of interest.

Acknowledgments

Research for this paper was supported by the National Natural Science Foundation of China (No. 42004089), the Major National Oil & Gas Specific Project of China (No. 2016ZX05050008), the Natural Science Foundation of Xinjiang Uygur Autonomous Region (No. 2017D01B57), the Natural Science Project of Xinjiang Uygur Autonomous Region Education Department (No. XJEDU2017S063, XJEDU2019Y070), the Young Elitist Scientific Research Project of China University of Petroleum, Beijing at Karamay (No. BJRC20170001), and the Scientific Research Starting Foundation of China University of Petroleum, Beijing at Karamay (No. RCYJ2016B-01-008).