Development and Validation of a GC-MS Method for the Detection and Quantification of Clotiapine in Blood and Urine Specimens and Application to a Postmortem Case

Table 1

Method validation parameters and data.

	Selectivity	Linearity ()	Accuracy (bias%)		Precision (RSD%)		LOD	LLOQ	Recovery (%)
			Low	High	Low	High			Low	High
Urine	No interference signals	0.9997	18	−0.6	14	3.2	1.2 ng/mL	3.9 ng/mL	103	99
Blood	No interference signals	0.9996	−18	−0.5	19	3.0	1.3 ng/mL	4.3 ng/mL	93	95