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International Journal of Analytical Chemistry
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International Journal of Analytical Chemistry
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2018
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Article
/
Tab 1
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Research Article
Simultaneous Determination of Cr, As, Se, and Other Trace Metal Elements in Seawater by ICP-MS with Hybrid Simultaneous Preconcentration Combining Iron Hydroxide Coprecipitation and Solid Phase Extraction Using Chelating Resin
Table 1
Operating conditions for the ICP-MS instrument.
ICP-MS: Agilent 7700x
Plasma conditions:
RF power
1.55 kW
Plasma gas flow rate
15.0 L min
−1
Ar
Auxiliary gas flow rate
0.90 L min
−1
Ar
Makeup gas flow rate
0 L min
−1
Ar
Carrier gas flow rate
1.05 L min
−1
Ar
Sampling depth (mm from load coil)
8.0 mm
Cell gas
He mode:4.3 mL min
−1
H
2
mode:6.0 mL min
−1
Nebulizer
Micro Mist
Sample uptake rate
0.45 mL min
−1
Data acquisition:
Accumulation time
0.3-1.0 s / point
Data point
3 points / peak
Repetition
3 times