Research Article

Rapid and Sensitive Determination of Methylxanthines in Commercial Brands of Tea Using Ultra-High-Performance Liquid Chromatography-Mass Spectrometry

Table 5

Recovery and repeatability of the proposed analytical method at three different spiking levels.

Concentration (μg/mL)Mean recovery (%) ± %RSD (n = 3)
TheobromineTheophyllineCaffeine

0.186.9 ± 3.683.4 ± 2.282.4 ± 3.7
1.095.7 ± 1.696.6 ± 1.093.7 ± 1.1
3.095.7 ± 1.694.1 ± 1.696.2 ± 2.3