International Journal of Analytical Chemistry / 2020 / Article / Tab 3 / Research Article
Simultaneous Quantitative Determination of Polyphenolic Compounds in Blumea balsamifera (Ai-Na-Xiang, Sembung) by High-Performance Liquid Chromatography with Photodiode Array Detector Table 3 Recovery of the targets (n = 3).
No. Original (mg) Spiked (mg) Found (mg) Recovery (%)a RSD (%)b 1 0.36 0.23 0.59 100.95 ± 3.95 3.91 0.30 0.29 0.61 104.00 ± 2.67 2.56 0.24 0.35 0.59 102.15 ± 3.37 3.30 2 0.33 0.21 0.55 102.84 ± 4.08 3.97 0.28 0.26 0.56 104.51 ± 2.94 2.81 0.22 0.32 0.54 102.64 ± 2.41 2.34 3 0.32 0.20 0.52 103.76 ± 3.67 3.54 0.27 0.24 0.53 105.68 ± 3.02 2.86 0.21 0.29 0.51 103.49 ± 2.38 2.30 4 2.40 1.67 4.02 96.90 ± 4.18 4.31 2.04 2.09 4.12 99.95 ± 2.63 2.63 1.60 2.50 4.09 99.53 ± 2.31 2.32 5 0.54 0.33 0.88 100.70 ± 4.80 4.76 0.46 0.41 0.89 103.53 ± 3.67 3.55 0.36 0.50 0.87 102.48 ± 3.64 3.56 6 0.11 0.06 0.17 103.95 ± 4.36 4.19 0.10 0.07 0.17 106.42 ± 0.32 0.30 0.08 0.09 0.17 109.92 ± 0.51 0.46 7 0.74 0.44 1.21 104.71 ± 1.64 1.57 0.63 0.55 1.17 96.69 ± 3.77 3.89 0.50 0.67 1.13 95.37 ± 2.22 2.32 8 0.10 0.05 0.16 108.99 ± 3.63 3.33 0.09 0.06 0.16 108.76 ± 0.88 0.81 0.07 0.08 0.15 107.31 ± 1.03 0.96 9 0.03 0.03 0.05 103.56 ± 2.84 2.74 0.02 0.03 0.06 109.35 ± 0.45 0.41 0.02 0.04 0.06 104.19 ± 0.37 0.36 10 0.05 0.03 0.08 101.56 ± 3.61 3.56 0.04 0.04 0.08 108.86 ± 1.50 1.38 0.03 0.04 0.08 107.88 ± 0.30 0.27 11 0.10 0.07 0.17 102.90 ± 4.55 4.42 0.09 0.09 0.18 104.61 ± 3.51 3.36 0.07 0.10 0.18 103.53 ± 2.47 2.39 12 0.84 0.53 1.39 102.48 ± 4.30 4.20 0.72 0.67 1.41 104.43 ± 3.43 3.28 0.56 0.80 1.39 103.05 ± 2.48 2.41 13 0.67 0.45 1.13 102.81 ± 4.19 4.08 0.57 0.56 1.16 104.67 ± 3.05 2.91 0.45 0.67 1.14 103.34 ± 2.43 2.36 14 0.24 0.13 0.36 97.59 ± 3.55 3.64 0.20 0.16 0.36 102.75 ± 1.42 1.39 0.16 0.19 0.36 106.26 ± 0.52 0.49 15 0.02 0.02 0.04 103.40 ± 4.19 4.05 0.02 0.02 0.04 104.65 ± 3.03 2.90 0.01 0.02 0.04 100.95 ± 2.78 2.76 16 0.19 0.12 0.31 95.85 ± 2.17 2.26 0.16 0.16 0.31 95.64 ± 2.64 2.76 0.13 0.19 0.31 95.03 ± 2.21 2.33 17 0.01 0.02 0.03 105.40 ± 0.99 0.93 0.01 0.02 0.03 107.31 ± 0.15 0.14 0.01 0.03 0.03 109.30 ± 0.52 0.47 18 0.03 0.02 0.05 104.16 ± 4.70 4.52 0.03 0.03 0.05 105.74 ± 3.09 2.93 0.02 0.03 0.05 105.15 ± 2.54 2.42
a Recovery% = [(found amount−original amount)/spiked amount] × 100%. b RSD% = (SD/mean) × 100%.