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International Journal of Photoenergy
Volume 2013 (2013), Article ID 726872, 6 pages
Research Article

Synthesis, Characterization, and Photocatalysis of Well-Dispersible Phase-Pure Anatase TiO2 Nanoparticles

College of Biological and Environmental Engineering, Zhejiang University of Technology, No. 18 ChaoWang Road, Hangzhou 310014, China

Received 7 February 2013; Accepted 29 March 2013

Academic Editor: Gang Liu

Copyright © 2013 Xiuzhen Wei et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.


High-purity anatase TiO2 nanoparticles were prepared using an improved sol-hydrothermal method. The as-prepared sample was characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), Brunauer-Emmett-Teller (BET), and UV-vis diffuse reflectance spectra. TEM results showed that the average particle size of all TiO2 particles was calculated to be () nm. The XRD analysis indicated that the present sample was fully crystallized and appeared to be highly phase-pure anatase. The BET analysis showed that the as-prepared sample had a very large specific surface area of 186.25 m2/g. The photocatalytic performance of TiO2 nanoparticles was evaluated by photocatalytic degradation of X-3B and X-BR solutions. The degradation results revealed that the as-prepared TiO2 showed slightly higher photocatalytic activities than P25. Whereas, the as-synthesized TiO2 can settle down and be separated easily after the photocatalytic reaction finishes.