Research Article
Optimization of Oil Yield from the Macro Algae Spirogyra by Solvent Extraction Process Using RSM and ANN
Table 2
The CCD arrived with Design-Expert factorial design and the response values.
| Exp. no | Particle size | Dryness level | Solid to solvent ratio | Reaction time | Extraction temperature | Oil yield % | | | | | | Experimental value | Predicted value | μm | % | g/ml | Hours | °C | RSM | ANN |
| 1 | − 1 | -1 | +1 | − 1 | − 1 | 22.13 | 22.42 | 22.15 | 2 | − 1 | +1 | − 1 | +1 | − 1 | 20.97 | 21.44 | 20.98 | 3 | − 1 | -1 | +1 | +1 | − 1 | 23.05 | 23.06 | 22.95 | 4 | − 1 | +1 | +1 | − 1 | − 1 | 22.61 | 22.90 | 22.64 | 5 | − 1 | +1 | − 1 | − 1 | 1 | 21.56 | 21.71 | 21.59 | 6 | − 1 | +1 | − 1 | − 1 | − 1 | 20.05 | 20.22 | 19.86 | 7 | − 1 | +1 | − 1 | +1 | +1 | 23.19 | 22.98 | 23.46 | 8 | − 1 | − 1 | +1 | − 1 | +1 | 23.58 | 23.30 | 23.60 | 9 | − 1 | +1 | +1 | − 1 | +1 | 23.48 | 23.52 | 23.52 | 10 | − 1 | − 1 | +1 | +1 | +1 | 23.53 | 24.00 | 23.54 | 11 | − 1 | − 1 | − 1 | +1 | − 1 | 20.49 | 20.81 | 20.53 | 12 | − 1 | +1 | +1 | +1 | − 1 | 23.53 | 23.56 | 23.55 | 13 | − 1 | − 1 | − 1 | − 1 | +1 | 21.03 | 21.36 | 21.06 | 14 | − 1 | 0 | 0 | 0 | 0 | 23.63 | 24.31 | 23.65 | 15 | − 1 | − 1 | − 1 | +1 | +1 | 22.71 | 22.62 | 22.75 | 16 | − 1 | − 1 | − 1 | − 1 | − 1 | 19.57 | 19.61 | 19.73 | 17 | − 1 | +1 | +1 | +1 | +1 | 23.59 | 24.23 | 23.61 | 18 | 0 | 0 | 0 | 0 | − 1 | 23.26 | 22.87 | 23.27 | 19 | 0 | 0 | 0 | − 1 | 0 | 23.98 | 24.78 | 24.00 | 20 | 0 | 0 | 0 | 0 | 0 | 24.78 | 25.42 | 25.20 | 21 | 0 | 0 | − 1 | 0 | 0 | 24.04 | 24.48 | 24.07 | 22 | 0 | 0 | 0 | +1 | 0 | 26.10 | 25.80 | 26.12 | 23 | 0 | 0 | +1 | 0 | 0 | 26.58 | 26.65 | 26.54 | 24 | 0 | 0 | 0 | 0 | 0 | 25.23 | 25.42 | 25.20 | 25 | 0 | 0 | 0 | 0 | 0 | 25.58 | 25.42 | 25.20 | 26 | 0 | − 1 | 0 | 0 | 0 | 24.41 | 25.11 | 24.44 | 27 | 0 | 0 | 0 | 0 | 0 | 25.70 | 25.42 | 25.20 | 28 | 0 | 0 | 0 | 0 | 0 | 24.83 | 25.42 | 25.20 | 29 | 0 | 0 | 0 | 0 | 0 | 24.90 | 25.42 | 25.20 | 30 | 0 | +1 | 0 | 0 | 0 | 25.72 | 25.52 | 25.75 | 31 | 0 | 0 | 0 | 0 | 0 | 25.35 | 25.42 | 25.20 | 32 | 0 | 0 | 0 | 0 | +1 | 23.46 | 24.30 | 23.48 | 33 | 0 | 0 | 0 | 0 | 0 | 25.41 | 25.42 | 25.20 | 34 | +1 | +1 | +1 | − 1 | +1 | 22.82 | 22.80 | 22.83 | 35 | +1 | − 1 | +1 | +1 | +1 | 23.44 | 23.44 | 23.44 | 36 | +1 | +1 | − 1 | − 1 | − 1 | 18.81 | 18.80 | 18.89 | 37 | +1 | − 1 | − 1 | +1 | − 1 | 19.25 | 19.56 | 19.27 | 38 | +1 | +1 | +1 | +1 | − 1 | 22.29 | 22.55 | 22.32 | 39 | +1 | +1 | − 1 | +1 | +1 | 21.96 | 22.11 | 21.97 | 40 | +1 | − 1 | +1 | − 1 | − 1 | 20.89 | 21.31 | 20.91 | 41 | +1 | − 1 | +1 | +1 | − 1 | 21.81 | 22.08 | 21.83 | 42 | +1 | +1 | − 1 | +1 | − 1 | 19.72 | 20.15 | 19.74 | 43 | +1 | − 1 | − 1 | − 1 | − 1 | 18.34 | 18.22 | 18.38 | 44 | +1 | +1 | +1 | − 1 | − 1 | 21.35 | 21.75 | 21.38 | 45 | +1 | +1 | +1 | +1 | +1 | 23.34 | 23.64 | 23.35 | 46 | +1 | − 1 | 1 | − 1 | +1 | 22.34 | 22.61 | 22.44 | 47 | +1 | − 1 | − 1 | +1 | +1 | 21.47 | 21.77 | 21.48 | 48 | +1 | 0 | 0 | 0 | 0 | 23.54 | 23.32 | 23.65 | 49 | +1 | +1 | − 1 | − 1 | +1 | 20.26 | 20.71 | 20.28 | 50 | +1 | − 1 | − 1 | − 1 | +1 | 20.37 | 20.38 | 19.88 |
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