Research Article
Correlation of Polymerization Conditions with Thermal and Mechanical Properties of Polyethylenes Made with Ziegler-Natta Catalysts
Table 3
DSC analysis for polyethylene samples.
| Sample | | | Temp. | Time | | | % crystallinity | (bar) | (bar) | (°C) | (hour) | (°C) | (°C) | (Cooling) |
| 1 | 5 | 0 | 60 | 0.5 | | | | 2 | 5 | 0 | 60 | 1 | | | | 3 | 5 | 0 | 80 | 0.5 | | | | 4 | 5 | 0 | 80 | 1 | | | | 5 | 5 | 2 | 60 | 0.5 | | | | 6 | 5 | 2 | 60 | 1 | | | | 7 | 5 | 2 | 80 | 0.5 | | | | 8 | 5 | 2 | 80 | 1 | | | | 9 | 5 | 5 | 60 | 0.5 | | | | 10 | 5 | 5 | 60 | 1 | | | | 11 | 5 | 5 | 80 | 0.5 | | | | 12 | 5 | 5 | 80 | 1 | | | | 13 | 10 | 0 | 60 | 0.5 | | | | 14 | 10 | 0 | 60 | 1 | | | | 15 | 10 | 0 | 80 | 0.5 | | | | 16 | 10 | 0 | 80 | 1 | | | | 17 | 10 | 2 | 60 | 0.5 | | | | 18 | 10 | 2 | 60 | 1 | | | | 19 | 10 | 2 | 80 | 0.5 | | | | 20 | 10 | 2 | 80 | 1 | | | | 21 | 10 | 5 | 60 | 0.5 | | | | 22 | 10 | 5 | 60 | 1 | | | | 23 | 10 | 5 | 80 | 0.5 | | | | 24 | 10 | 5 | 80 | 1 | | | |
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