Research Article

Optimization of Process Variables in the Synthesis of Tributyl Citrate Using a Polyvinylpolypyrrolidone-Supported Brønsted Acidic Ionic Liquid Catalyst

Figure 6

Reusability of the [BsPVPP]HSO4 catalyst for the esterification of citric acid with n-butanol. Reaction conditions: citric acid, 0.06 mol; n-butanol, 0.31 mol; catalyst, 6.6 wt%; temperature, 120°C; time, 5.5 h.