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Journal of Automatic Chemistry
Volume 11, Issue 5, Pages 227-234
http://dx.doi.org/10.1155/S1463924689000453

Computer-controlled apparatus for automated development of continuous flow methods

1Department of Chemistry, University of British Columbia, Vancouver V6T 1Y6, Canada
2BP Research Centre, Chertsey Road, Sunbury-on-Thames TW16 7LM, UK
3Grace Service Chemicals, Foundry Lane, Widnes WA8 8UD, UK
4Department of Chemistry, Dalhousie University, Halifax, Nova Scotia B3H 4J3, Canada

Copyright © 1989 Hindawi Publishing Corporation. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Abstract

An automated apparatus to assist in the development of analytical continuous flow methods is described. The system is capable of controlling and monitoring a variety of pumps, valves, and detectors through an IBM PC-AT compatible computer. System components consist of two types of peristaltic pumps (including a multiple pump unit), syringe pumps, electrically and pneumatically actuated valves, and an assortment of spectrophotometric and electrochemical detectors. Details of the interface circuitry are given where appropriate. To demonstrate the utility of the system, an automatically generated response surface is presented for the flow injection determination of iron(II) by its reaction with 1,10-phenanthroline.