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Journal of Analytical Methods in Chemistry
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Journal of Analytical Methods in Chemistry
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2012
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Article
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Tab 4
Research Article
Direct Quantitative Analysis of Arsenic in Coal Fly Ash
Table 4
Optimized furnace program for the analysis of raw coal (liquid sampling system).
Step
Parameters
Ar gas
Temperature (°C)
Rate (°C s
−1
)
Hold time (s)
Total time (s)
Drying
90
30
5
7.3
Max
Drying
105
10
20
21.5
Max
Drying
120
10
5
6.5
Max
Pyrolysis
1500
100
30
43.8
Max
Autozero (AZ)
1500
0
6
6.0
Stop
Atomization
2500
1000
6
7.0
Stop
Cleaning
2600
1000
10
10.1
Max