Effects of Iron Concentration Level in Extracting Solutions from Contaminated Soils on the Determination of Zinc by Flame Atomic Absorption Spectrometry with Two Background Correctors
Table 1
Sequential extraction procedure (from Rauret et al. [33]).
Steps
Extracting solutions
Nominal target phases
1
Acetic acid 0.11 M
Fraction F1: exchangeable, water- and acid-soluble
2
Hydroxylamine + hydrochloric acid 0.50 M at pH 2
Fraction F2: reducible
3
Hydrogen peroxide 8.8 M, + ammonium acetate 1.0 M at pH 2