Journal of Analytical Methods in Chemistry / 2012 / Article / Tab 3 / Research Article
Effects of Iron Concentration Level in Extracting Solutions from Contaminated Soils on the Determination of Zinc by Flame Atomic Absorption Spectrometry with Two Background Correctors Table 3 Pseudototal Fe, Cu, and Zn concentrations (mean value ± standard deviation) measured in certified reference soil (
𝑛
=
3
) and kitchen garden (KG) soil samples (
𝑛
=
3
).
Samples Fe in this work (mg kg−1 ) Cu in this work (mg kg−1 ) Zn certified value (mg kg−1 ) Zn with the D2 method (mg kg−1 ) Zn with the HSSR method (mg kg−1 ) BCR-483 26,642 ± 1,180a 403 ± 11c 987 ± 37b,c 939 ± 48 1,013 ± 59 BCR-701 36,975 ± 342d 43.8 ± 1.5e 454 ± 19f 474 ± 15 478 ± 7 KG1 22,496 ± 717
3
5
.
5
±
2
.
3
821 ± 10 808 ± 6 KG2 24,681 ± 799
2
5
.
6
±
1
.
9
513 ± 4 531 ± 7 KG3 23,628 ± 685
1
3
.
3
±
1
.
3
813 ± 15 958 ± 17 KG4 18,846 ± 578
7
8
.
2
±
3
.
1
867 ± 9 895 ± 1 KG5 20,026 ± 624
7
4
.
4
±
2
.
8
1,052 ± 21 1,051 ± 12 KG6 24,399 ± 790
6
3
.
3
±
2
.
3
1,398 ± 21 1,410 ± 24 KG7 18,851 ± 580
2
7
.
3
±
1
.
1
505 ± 3 522 ± 6 KG8 27,029 ± 890
1
7
0
.
4
±
5
.
4
4,502 ± 25 4,842 ± 54 KG9 31,440 ± 661
1
2
.
6
±
1
.
0
655 ± 5 667 ± 5
a From Kubová et al. [38 ], [Fe] = 26,700 ± 480 mg kg−1 .
b Indicative value from Rauret et al. [39 ], (
𝑛
=
5
).
c From Pueyo et al. [40 ], [Zn] = 1,026 ± 37 mg kg−1 ; [Cu] = 373 ± 14 mg kg−1 (
𝑛
=
6
).
d From Kubová et al. (2004) [38 ], [Fe] = 38,580 ± 220 mg kg−1 .
e Certified value: [Cu] =
4
6
.
4
±
1
.
8
mg kg−1 (
𝑛
=
6
).
f From Pueyo et al. [40 ], [Zn] = 474 ± 10 mg kg−1 (
𝑛
=
6
).