Research Article

Orthogonal Design Study on Factors Affecting the Determination of Common Odors in Water Samples by Headspace Solid-Phase Microextraction Coupled to GC/MS

Table 4

The basic analytical results of the orthogonal experiment design L32 (49).

Compounds (×107)K valueFactorsa
ABCDEFG

2-MIB 13.43713.19318.28018.92117.17319.49718.747
18.12320.02417.81818.35020.66618.50019.563
24.05321.31720.40020.33518.39018.95619.176
21.52022.59920.63519.52720.90420.18019.647

GSM 44.44243.07669.66968.58763.48168.59667.181
58.09076.95963.10165.58770.95963.79369.662
73.29674.00965.21069.95667.34166.74569.415
97.63379.41775.48169.33171.68074.32767.203

Factor A: extraction temperature (°C); Factor B: extraction time (min); Factor C: rotate-speed (rpm); Factor D: ionic strength (w/v, %); Factor E: desorption time (min); Factor F: desorption temperature (°C); and Factor G: solution pH.