Adsorptive Cathodic Stripping Voltammetric Determination of Cefoperazone in Bulk Powder, Pharmaceutical Dosage Forms, and Human Urine

Table 1

Variable ranges used in the optimization process of voltammetric measurements of 0.03 μg/mL cefoperazone.

Variable	DP-AdCSV	SW-AdCSV
Accumulation time	100→120 s
Pulse amplitude	0.05→0.1 V
Pulse time	0.02→0.04 s
Frequency		60→80 Hz
Voltage step	0.01→0.02 V	0.005→0.007 V
Voltage step time	0.05→0.06 s