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Journal of Analytical Methods in Chemistry
Volume 2014, Article ID 976145, 6 pages
http://dx.doi.org/10.1155/2014/976145
Research Article

Preparation and Characterization of an Amphipathic Magnetic Nanosphere

1College of Pharmacy, Henan University of Traditional Chinese Medicine, Zhengzhou 450000, China
2Key Laboratory of Nonferrous Metal Chemistry and Resources Utilization of Gansu Province, Lanzhou University, Lanzhou 730000, China

Received 24 November 2013; Accepted 4 January 2014; Published 5 March 2014

Academic Editor: Xiu-Ping Yan

Copyright © 2014 Yongsheng Ji et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Abstract

The amphipathic magnetic nanospheres were synthesized using C8 and polyethylene glycol as ligands. Their morphology, structure, and composition were characterized by transmission electron microscope, Fourier transform infrared, and elementary analysis. The prepared materials presented uniform sphere with size distribution about 200 nm. The magnetic characteristics of magnetic nanomaterials were measured by vibrating sample magnetometer. The target products had a saturation magnetization value of 50 emu g−1 and superparamagnetism. The adsorption capability was also studied by static tests, and the material was applied to enrich benzenesulfonamide from calf serum. The results exhibited that the C8-PEG phase owned better adsorption capability, biocompatible property, and dispersivity in aqueous samples.