Headspace-Solid-Phase Microextraction-Gas Chromatography as Analytical Methodology for the Determination of Volatiles in Wild Mushrooms and Evaluation of Modifications Occurring during Storage

Table 3

Validation data for predominant volatiles of Agaricus bisporus: linear regression data, limit of detection (LOD), limit of quantification (LOQ), and recovery values (average of three analyses).

Compound	Linear range (ppb) for DVB/Car/PDMS fiber	Linear range (ppb) for PDMS/DVB fiber		Regression equation	LOD (ppb); S/N = 3	LOQ (ppb); S/N = 10	Recovery (±RSD) %; (10 ppb spiked)
3-Octanone	156.25–1,250.00	39.06–10,000.00	0.9959		0.8	3.2	98.2 ± 2.1
3-Octanol	78.12–2,500.00	39.06–10,000.00	0.9594		1.6	2.7	97.6 ± 2.3
Benzyl alcohol	78.12–625.00	78.12–2,500.00	0.9965		1.1	3.9	114.3 ± 3.2
(2E)-Octenol	156.25–1,250.00	78.12–10,000.00	0.9988		0.7	4.2	94.8 ± 1.1