Research Article
Simultaneous Determination of Six Active Compounds in Yixin Badiranjibuya Granules, a Traditional Chinese Medicine, by RP-HPLC-UV Method
Table 6
Recovery test for the determination of the investigated analytes (mean ± SD,
).
| Analytes | Originals (mg) | Spiked (mg) | Found (mg) | Recovery (%) | RSD (%) |
| LLD | 0.6209 | 0.3184 | 0.9344 ± 0.0036 | 98.43 ± 1.10 | 1.12 | 0.6368 | 1.2483 ± 0.0047 | 98.53 ± 0.72 | 0.73 | 0.9552 | 1.5667 ± 0.0101 | 99.00 ± 1.05 | 1.06 |
| AGD | 0.2347 | 0.1165 | 0.3508 ± 0.0021 | 99.63 ± 1.80 | 1.81 | 0.2330 | 0.4678 ± 0.0033 | 100.06 ± 1.44 | 1.44 | 0.3495 | 0.5849 ± 0.0037 | 100.20 ± 1.05 | 1.05 |
| RA | 0.7057 | 0.3276 | 1.0280 ± 0.0033 | 98.33 ± 1.01 | 1.02 | 0.6552 | 1.3565 ± 0.0106 | 99.34 ± 1.59 | 1.60 | 0.9828 | 1.6867 ± 0.0056 | 99.80 ± 0.59 | 0.59 |
| DTD | 0.8085 | 0.4176 | 1.2258 ± 0.0016 | 99.88 ± 0.41 | 0.41 | 0.8352 | 1.6528 ± 0.0085 | 101.09 ± 1.02 | 1.01 | 1.2528 | 2.0573 ± 0.0123 | 99.66 ± 1.00 | 1.00 |
| TLN | 0.9779 | 0.3950 | 1.3696 ± 0.0009 | 99.10 ± 0.19 | 0.19 | 0.9875 | 1.9715 ± 0.0071 | 100.63 ± 0.75 | 0.74 | 1.5800 | 2.5592 ± 0.0059 | 100.06 ± 0.38 | 0.38 |
| ATD | 0.9535 | 0.4680 | 1.4236 ± 0.0073 | 100.41 ± 1.53 | 1.52 | 0.9360 | 1.8888 ± 0.0168 | 99.93 ± 1.79 | 1.79 | 1.4040 | 2.3670 ± 0.0166 | 100.66 ± 1.20 | 1.19 |
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