Research Article

Total Arsenic, Cadmium, and Lead Determination in Brazilian Rice Samples Using ICP-MS

Table 3

LOD, LOQ, working range, and correlation coefficient of calibration curve for the microwave digestion method.

Parameters (unit)AsCdPb

LOD (mg kg−1)0.0110.0120.030
LOQ (mg kg−1)0.0380.0400.064
Working range (µg L−1)1–401.2–241–20
Correlation coefficient of the calibration curve0.99970.99970.9991, 0.9991, 0.9992

For Pb, calculated as the mean values among the three measured isotopes cited in Table 1.