Research Article
A Simple and Quick Method for the Determination of Pesticides in Environmental Water by HF-LPME-GC/MS
Table 2
Analytical performance of GC/MS method using HF-LPME for the extraction of pesticides in environmental water.
| Pesticide | Quantification ion (m z−1) | Linearity () | Precision RSD (%) | Recovery (%) | LOD (µg L−1) | LOQ (µg L−1) |
| Parathion-methyl | 263 | 0.9932 | 2.80 | 110.05 | 0.04 | 0.14 | Chlorpyrifos | 97 | 0.9950 | 3.98 | 114.73 | 0.44 | 1.46 | Captan | 79 | 0.9955 | 14.98 | 100.65 | 0.20 | 0.67 | Procymidone | 67 | 0.9996 | 4.77 | 113.68 | 0.17 | 0.57 | α-Endosulfan | 195 | 0.9903 | 6.50 | 110.75 | 0.12 | 1.69 | Prothiofos | 113 | 0.9990 | 0.90 | 112.17 | 0.35 | 1.16 | Cyproconazole | 125 | 0.9943 | 9.31 | 85.17 | 0.14 | 0.48 | Ethion | 125 | 0.9807 | 2.36 | 113.36 | 0.13 | 0.42 | Triazophos | 161 | 0.9906 | 13.56 | 91.08 | 0.09 | 0.31 | Phosmet | 160 | 0.9874 | 15.16 | 111.10 | 0.23 | 0.76 |
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Compounds are listed in sequence of elution. Concentration 10 µg L−1; .
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