Research Article
Evaluation of the Influence of Sulfur-Fumigated Paeoniae Radix Alba on the Quality of Si Wu Tang by Chromatographic and Chemometric Analysis
Table 2
Linear regression data, LOD, LOQ, precisions, repeatabilities, and recoveries of ten marker compounds in SWT (n = 6).
| Analyte | Regression equation | | Linear range (µg/mL) | LOD (µg/mL) | LOQ (µg/mL) | Precision, RSD (%) | Repeatability RSD (%) | Recovery | Intraday | Interday | Average recovery (%) | RSD (%) |
| Gallic acid | | 0.9990 | 11.30–182.00 | 1.70 | 5.65 | 1.10% | 1.9% | 2.16% | 99.67 | 1.31 | 5-Hydroxymethylfurfural | | 0.9994 | 4.00–64.40 | 0.02 | 0.06 | 0.26% | 0.43% | 1.77% | 101.58 | 1.25 | Cianidanol | | 0.9990 | 14.00–239.00 | 0.53 | 1.75 | 0.49% | 0.59% | 3.03% | 101.37 | 2.17 | Albiflorin | | 0.9988 | 49.00–789.00 | 3.71 | 12.25 | 1.44% | 2.12% | 2.72% | 98.45 | 2.33 | Paeoniflorin | | 0.9990 | 22.30–357.00 | 1.69 | 5.57 | 2.00% | 2.31% | 2.92% | 102.75 | 1.78 | Ferulic acid | | 0.9991 | 1.06–17.00 | 0.02 | 0.07 | 0.38% | 1.05% | 2.86% | 99.63 | 1.15 | Verbascoside | | 0.9994 | 3.80–61.00 | 0.15 | 0.48 | 2.73% | 2.82% | 2.87% | 98.69 | 2.73 | Senkyunolide I | | 0.9998 | 4.80–78.00 | 0.04 | 0.15 | 0.35% | 0.54% | 2.97% | 102.55 | 2.06 | Senkyunolide A | | 0.9989 | 9.91–158.50 | 0.18 | 0.61 | 0.61% | 0.93% | 2.61% | 101.58 | 2.15 | Z-Ligustilide | | 0.9990 | 11.30–182.00 | 0.86 | 2.83 | 0.21% | 0.37% | 2.41% | 99.67 | 1.79 |
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