Simultaneous Determination of 5 Flavonoids and 7 Saponins for Quality Control of Traditional Chinese Medicine Preparation Xinnaoshutong Capsule Using HPLC-VWD-ELSD
Table 3
Contents of nine components of samples from different batches of XC (%).
Batch
2
4
5
6
8
9
10
11
12
Saponin%
Flavone%
20110101139
0.2906
1.4035
0.4596
0.0151
0.0193
0.0072
0.0006
0.0004
0.0002
2.1687
0.0277
20110106081
0.2852
1.3240
0.4343
0.0185
0.0193
0.0070
0.0008
0.0004
0.0003
2.0620
0.0278
20100407101
0.3683
1.3842
0.5486
0.0222
0.0251
0.0105
0.0016
0.0006
0.0005
2.3234
0.0382
20110201029
0.2853
1.4192
0.4698
0.0181
0.0195
0.0074
0.0006
0.0003
0.0003
2.1923
0.0281
20110402021
0.2871
1.5198
0.4869
0.0178
0.0157
0.0056
0.0014
0.0005
0.0005
2.3115
0.0238
20100703001
0.1632
0.5924
0.1899
0.0212
0.0049
0.0016
0.0069
0.0021
0.0018
0.9667
0.0173
20100104118
0.3555
1.4975
0.5163
0.0208
0.0093
0.0033
0.0009
0.0005
0.0004
2.3901
0.0143
20101002104
0.2628
1.4878
0.3785
0.0168
0.0067
0.0024
0.0006
0.0003
0.0003
2.1459
0.0102
20110903074
0.2694
1.5167
0.4212
0.0187
0.0226
0.0081
0.0028
0.0009
0.0007
2.2260
0.0352
20101102056
0.2936
1.4332
0.3244
0.0189
0.0096
0.0039
0.0017
0.0006
0.0006
2.0702
0.0164
20110207058
0.3138
1.3034
0.3977
0.0198
0.0158
0.0064
0.0010
0.0005
0.0004
2.0347
0.0241
20100104118
0.3574
1.4958
0.5284
0.0207
0.0094
0.0035
0.0007
0.0004
0.0004
2.4023
0.0143
20110201022
0.3093
1.2911
0.4090
0.0199
0.0158
0.6430
0.0010
0.0005
0.0004
2.0293
0.6607
20110402020
0.3398
1.6046
0.5140
0.0176
0.0165
0.0062
0.0014
0.0005
0.0005
2.4759
0.0250
20090211016
0.1005
1.1903
0.3912
0.0215
0.0361
0.0133
0.0034
0.0010
0.0009
1.7035
0.0547
20110101137
0.2997
1.4651
0.5239
0.0170
0.0231
0.0092
0.0013
0.0004
0.0005
2.3057
0.0345
20100705001
0.1797
0.7505
0.2193
0.0178
0.0067
0.0023
0.0069
0.0015
0.0016
1.1673
0.0190
20100407100
0.3665
1.3997
0.5504
0.0204
0.0248
0.0103
0.0018
0.0006
0.0006
2.3369
0.0381
20100303124
0.3381
1.2121
0.4165
0.0198
0.0275
0.0104
0.0030
0.0009
0.0007
1.9865
0.0426
20110303061
0.3196
1.6128
0.4647
0.0165
0.0202
0.0072
0.0013
0.0005
0.0004
2.4136
0.0296
20110303046
0.3419
1.6801
0.4776
0.0181
0.0210
0.0073
0.0010
0.0005
0.0005
2.5176
0.0303
20101002075
0.2652
2.3379
0.3929
0.0153
0.0070
0.0026
0.0007
0.0003
0.0002
3.0113
0.0108
20110903058
0.2944
1.6131
0.4548
0.0189
0.0233
0.0085
0.0033
0.0009
0.0008
2.3811
0.0368
20090211015
0.3568
1.3093
0.4059
0.0189
0.0412
0.0140
0.0037
0.0013
0.0010
2.0909
0.0612
20100908090
0.2750
1.5758
0.4243
0.0147
0.0161
0.0059
0.0015
0.0006
0.0005
2.2898
0.0245
20100303124
0.3086
1.1683
0.3987
0.0161
0.0285
0.0101
0.0032
0.0009
0.0007
1.8917
0.0434
20100908042
0.2952
1.5704
0.4392
0.0161
0.0156
0.0061
0.0016
0.0006
0.0004
2.3208
0.0242
20110201056
0.2678
1.3067
0.4850
0.0142
0.0221
0.0087
0.0019
0.0004
0.0005
2.0737
0.0336
20110106068
0.2813
1.4765
0.3453
0.0149
0.0108
0.0044
0.0017
0.0005
0.0005
2.1180
0.0179
20101102072
0.2723
1.2733
0.3775
0.0133
0.0193
0.0069
0.0008
0.0003
0.0004
1.9363
0.0278
0.052
0.19
0.05
0.05
0.0023
0.00081
ND
ND
0.00018
0.342
0.00329
0.055
0.069
0.044
0.06
0.0025
0.0009
ND
ND
0.00047
0.228
0.00387
Note: compounds 1, 3, and 7 were not detected in the XC; compounds 1, 3, 7, 10, and 11 were not detected in TT; ND: not detected. NM: TT sample from neimenggu province, AH: TT sample from Anhui province.
