Research Article

Nonvolatile Chemical Constituents from the Leaves of Ligusticopsis wallichiana (DC.) Pimenov & Kljuykov and Their Free Radical-Scavenging Activity

Table 4

1H- and13C-NMR spectroscopic data of compound 4 in CD3OD.

Carbon numberδH, mult. (J in Hz)δC

1126.6, Ca
2153.5, Cb
37.37, s98.3, CH
3a153.4, Cb
47.82, d (2.2)144.9, CH
56.81, d (2.2)106.2, CH
5a120.8, Ca
67.32, s120.6, CH
72.87, t (7.6)26.1, CH2
82.40, t (7.6)35.3, CH2
9174.8, C
Glc-14.82, d (7.3)101.5, CH
Glc-23.26–3.30, m73.3, CH
Glc-33.16, t (9.1)77.0, CHc
Glc-43.16, t (9.1)69.9, CH
Glc-53.26–3.30, m76.6, CHc
Glc-63.72, dd (5.0, 11.8)60.8, CH2
3.75, dd (1.8, 11.8)

a,b,cAssignments with the same superscripts may be interchanged in the same column.