Quality Analysis of Long dan Xie gan Pill by a Combination of Fingerprint and Multicomponent Quantification with Chemometrics Analysis

Table 4

Recovery results of four components in Long dan Xie gan pill samples.

Components	No.	Sampling amount (g)	Sample content (mg)	Added amount (mg)	Detected amount (mg)	Recovery (%)	Average recovery (%)
Gentiopicrin	1	1.0005	4.772	4.653	9.371	98.83	100.59% (RSD 1.22%)
	2	1.0017	4.778	4.653	9.432	100.02
	3	1.0006	4.773	4.653	9.431	100.11
	4	1.0047	4.792	4.653	9.473	100.60
	5	1.0030	4.784	4.653	9.528	101.96
	6	1.0026	4.782	4.653	9.529	102.02
Baicalin	1	1.0005	3.842	3.762	7.478	96.65	97.96% (RSD 0.87%)
	2	1.0017	3.847	3.762	7.537	98.09
	3	1.0006	3.842	3.762	7.503	97.32
	4	1.0047	3.858	3.762	7.583	99.02
	5	1.0030	3.852	3.762	7.543	98.11
	6	1.0026	3.850	3.762	7.554	98.56
Baicalein	1	1.0005	0.620	1.214	1.807	97.78	97.71% (RSD 0.72%)
	2	1.0017	0.621	1.214	1.802	97.28
	3	1.0006	0.620	1.214	1.793	96.62
	4	1.0047	0.623	1.214	1.809	97.69
	5	1.0030	0.622	1.214	1.816	98.35
	6	1.0026	0.622	1.214	1.818	98.52
Wogonin	1	1.0005	0.400	0.750	1.141	98.80	99.98% (RSD 1.29%)
	2	1.0017	0.401	0.750	1.146	99.33
	3	1.0006	0.400	0.750	1.141	98.80
	4	1.0047	0.402	0.750	1.153	100.13
	5	1.0030	0.401	0.750	1.156	100.67
	6	1.0026	0.401	0.750	1.167	102.13