Rapid Determination of Sotolon in Fortified Wines Using a Miniaturized Liquid-Liquid Extraction Followed by LC-MS/MS Analysis

Table 1

Performance results obtained for the proposed miniaturized liquid-liquid extraction method.

Parameter	Result
Linear regression	ASTL = 46437 [STL] + 43722
Linear concentration range (μg/L)	1.0–2000
R^2	0.9999
LOD (μg/L)	0.011
LOQ (μg/L)	0.037
Repeatability (% RSD)	3.4–6.4
Reproducibility (% RSD)	5.4–10.0
Recovery (%)
FW + STL 250 μg/L	92
FW + STL 1000 μg/L	98

A_STL, sotolon peak area; [STL], sotolon concentration in μg/L; LOD, limit of detection; LOQ, limit of quantification; FW, fortified wine; STL, sotolon.