Research Article

Determination of Cyclopropane Fatty Acids in Food of Animal Origin by 1H NMR

Table 1

Comparison of 1H NMR and GC-MS results on the presence of CPFAs in some representative samples of fat of animal origin.

SamplesNumber of analysed samplesCPFA (GC-MS) (mg/kg fat)CPFA (1H NMR) (mg/kg fat)

Cheese
Reference cheese600 ± 50690 ± 60
Parmigiano Reggiano5<LOD<LOD
Grana Padano5400–700400–800
Meat
Commercial bovine meat5200–400300–400
Bovine meat of certified origin (not fed with silages)2<LOD<LOD
Other meats (Pork and chicken)4<LOD<LOD
Cured meat
Salami160<LOD
Parma ham1120<LOD
Bresaola1340400
Fish
Eel2180–350400–590
Mullet1120800